Butylamine → HCID 178448795, compound

Participants

Reaction Steps

Follow a procedure similar to that of Preparation 2 except use n-butylamine (0.53 mL, 5.3406 mmol); toluene (7.0 mL); a solution of titanium(IV) chloride (0.1006 g, 0.5303 mmol) in toluene (3.0 mL); stir the resulting solution for 1 hour; then add a solution of 2-((1,1′:3′,1″-terphenyl)-2′-ylamino)-2-cyclohexen-1-one (0.3062 g, 0.9021 mmol, Preparation 7) in toluene (2.0 mL); toluene rinse (1.0 mL); to afford after isolation 0.3352 g (94.18%) of the product (J) as a brown oil.

Provenance & Evidence