HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Fluorophenyl)piperazine → HCID 68560962, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Fluorophenyl)piperazine | HCID 70529 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Sodium triacetoxyborohydride | HCID 5049666 | — |
| Reactant | HCID 86639953 | HCID 86639953 | — |
| Product | HCID 68560962 | HCID 68560962 | — |
Reaction Steps
121 mg (92%) of target compound was obtained by using a method same as in Example 1 by using 3-(1-phenyl-3-isobutyl-1H-pyrazol-5-yl)propanal (80 mg, 0.312 mmol), 1-(2-fluorophenyl)piperazine (56 mg, 0.312 mmol), DIPEA (0.082 mL, 0.468 mmol) and NaBH(OAc)3 (198 mg, 0.936 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08372844B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-50bd98a08498442c95576ffe3832b95b |
| Source note | uspto-grants-2013_02 |