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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 387314Generated: October 31, 2026

N-bromobutanimide → HCID 59332638, compound

https://huagongshe.com/reaction/387314

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-bromobutanimideHCID 67184—
ReactantHCID 59332581HCID 59332581—
SolventMethanolHCID 887—
SolventDichloromethaneHCID 6344—
ProductHCID 59332638HCID 59332638—

Reaction Steps

NBS (40 mg, 0.23 mmol) was added to a solution of 4-fluoro-2,3-dihydro-1H-indole-7-carboxylic acid (36 mg, 0.14 mmol) in DCM (3 mL) and MeOH (1 mL). The reaction was stirred at room temperature overnight and filtered. The filtrate was evaporated, and the residue was purified by flash chromatography, giving the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08372875B2
Source datasetuspto-grants-2013_02
ORD IDord-f209d9b8086042f5b6d3b1f1a3403b2a
Source noteuspto-grants-2013_02