HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Methylthio)propylamine → HCID 21949116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Methylthio)propylamine | HCID 77743 | — |
| Reactant | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 21949116 | HCID 21949116 | 93.08% |
Reaction Steps
3-Methylthiopropylamine (5.5 ml, 50 mmol) was used for reaction in the same manner as Production Example 310-1, and purification was performed by silica gel column chromatography (hexane/ethyl acetate system) to obtain the title compound (10.486 g, 46.54 mmol, 93.08%) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08372981B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-605ae7e7ae7846ce9545c50f5890b5b3 |
| Source note | uspto-grants-2013_02 |