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HRID388179

反应详情

EQUATION

反应方程式

HRID 388179 的结构方程式

REACTANTS

反应物

1
结构：COc1ccc2c3c1O[C@H]1C(=O)CC[C@H]4[C@@H](C2)N(C)CC[C@]314.O=C(O)C(O)C(O)C(=O)O
HCID20831824

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c3c1O[C@H]1C(=O)CC[C@H]4[C@@H](C2)N(C)CC[C@]314
HCID5284569

Hydrocodone

C18H21NO3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

Hydrocodone polistirex was prepared by mixing 4.00 kg of hydrocodone bitartrate with 4.76 kg of ion-exchange resin particles (ABMERLITE IRP69; US Std. Mesh #100-#400) suspended in USP water at about 70° C. The resulting suspension was centrifuged and the product washed with USP water. The wet cake was dried and sieved through a US Std #30 mesh screen. The hydrocodone content of the dried product was equivalent to approximately 56% by weight of hydrocodone bitartrate.

WORKUP

后处理

  1. washthe product washed with USP water
  2. customThe wet cake was dried
  3. filtrationsieved through a US Std #30 mesh screen