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HRID388672

反应详情

EQUATION

反应方程式

HRID 388672 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2c(Cl)cc(Cl)nc2c1C
HCID53400954

2,4-Dichloro-7-methoxy-8-methylquinoline

C11H9Cl2NO

结构：COc1ccc(COc2cc(Cl)nc3c(Cl)c(OC)ccc23)cc1
HCID56605153

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(COc2cc(Cl)nc3c(C)c(OC)ccc23)cc1
HCID56605159

未命名化合物

收率 50%

PROCEDURE

实验过程

2-Chloro-8-methyl-7-methoxy-4-(4-methoxy-benzyloxy)-quinoline 221b was synthesized from compound 220b as a white powder in 50% yield, following the procedure as described for compound 221d. 1H NMR (CDCl3, 376 MHz) δ (ppm) 2.60 (s, 3H), 3.85 (s, 3H), 3.97 (s, 3H), 5.18 (s, 2H), 6.69 (s, 1H), 6.97 (d, J=8.57 Hz, 1H), 7.19 (d, J=8.57 Hz, 1H), 7.42 (d, J=8.57 Hz, 1H), 8.02 (d, J=8.57 Hz, 1H).