HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetamide → Carboxyamidotriazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetamide | HCID 7898 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,5-Dichloro-4-(4-chlorobenzoyl)benzyl azide | HCID 13649662 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Carboxyamidotriazole | HCID 108144 | — |
Reaction Steps
3,5-dichloro-4-(4′-chlorobenzoyl)benzyl azide (858.D) (1 mole) is reacted with cyanoacetamide (1.69 mole) in hot Acetonitrile, and Potassium carbonate, (6.2 mole) to give 5-amino-1-(4-(4-chlorobenzoyl)-3,5-dichlorobenzyl)-1,2,3-triazole-4-carboxamide (858.E).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08377973B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-ea5ad1f3fb854cef84328d47b7185d85 |
| Source note | uspto-grants-2013_02 |