HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Diamino-2-methylbenzoic acid → HCID 178497378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Diamino-2-methylbenzoic acid | HCID 135524 | — |
| Reactant | 2-Isopropylphenyl isothiocyanate | HCID 142052 | — |
| Product | HCID 178497378 | HCID 178497378 | — |
Reaction Steps
1-Isopropyl-2-isothiocyanatobenzene (5 mmol) and methyl 3,4-diaminobenzoate (5 mmol) were reacted, following general procedure B, to yield 2-(2-Isopropylphenylamino)-1H-benzimidazole-5-carboxylic acid methyl ester, which was purified by silica gel chromatography using DCM/ethyl acetate as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08377983B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-4cd2e31413bc43a38e84dd3f9e767206 |
| Source note | uspto-grants-2013_02 |