HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-1-isothiocyanatobenzene → HCID 68446627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-1-isothiocyanatobenzene | HCID 81066 | — |
| Reactant | 3,5-Diamino-2-methylbenzoic acid | HCID 135524 | — |
| Product | HCID 68446627 | HCID 68446627 | — |
Reaction Steps
2,4-Dichloro-1-isothiocyanatobenzene (5 mmol) and methyl 3,4-diaminobenzoate (5 mmol) were reacted, following general procedure B, to yield 2-(2,4-dichlorophenylamino)-3H-benzimidazole-5-carboxylic acid methyl ester, which was purified by silica gel chromatography using DCM/ethyl acetate as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08377983B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-b6b626722bcd4cb5998f70412adf8981 |
| Source note | uspto-grants-2013_02 |