HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Diamino-2-methylbenzoic acid → HCID 68445131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Diamino-2-methylbenzoic acid | HCID 135524 | — |
| Reactant | 2-Ethylphenyl isothiocyanate | HCID 2796213 | — |
| Product | HCID 68445131 | HCID 68445131 | — |
Reaction Steps
2-Ethyl-1-isothiocyanatobenzene (3 mmol) and methyl 3,4-diaminobenzoate (3 mmol) were reacted, following general procedure B, to yield 2-(2-ethylphenylamino)-3H-benzimidazole-5-carboxylic acid methyl ester, which was purified by silica gel chromatography using DCM/ethyl acetate as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08377983B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-9488a390e0754e3e8839136c9c56d7c5 |
| Source note | uspto-grants-2013_02 |