Butylamine → HCID 44469873, compound

HRID 38916Notes

Reaction equation

HRID 38916 reaction equation
CC1C=CC(S(O[CH2:12][CH:13]2[O:18][C:17]3[CH:19]=[C:20]([S:23]([CH3:26])(=[O:25])=[O:24])[CH:21]=[CH:22][C:16]=3[O:15][CH2:14]2)(=O)=O)=CC=1.[CH2:27]([NH2:31])[CH2:28][CH2:29][CH3:30]>C(#N)C>[CH3:26][S:23]([C:20]1[CH:21]=[CH:22][C:16]2[O:15][CH2:14][CH:13]([CH2:12][NH:31][CH2:27][CH2:28][CH2:29][CH3:30])[O:18][C:17]=2[CH:19]=1)(=[O:24])=[O:25]

Participants

4

Reactant 2

HCID 8007ButylamineHCID 86652933[7-(Methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-yl]methyl 4-methylbenzenesulfonate

Product 1

HCID 44469873HCID 44469873, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

Preparation according to Example 25 using [7-(methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-yl]methyl 4-methylbenzenesulfonate (0.018 g, 0.046 mmol), butan-1-amine (0.5 ml), ACN (3 ml). MS m/z (rel. intensity, 70 eV) 299 (M+, 6), 256 (5), 87 (6), 86 (bp), 70 (5).

Workup

  1. customPreparation

Sources & evidence

ORD record
ord-e4bed67b92f94c12a8a588779093e7fe
Source dataset
uspto-grants-2013_09
Patent number
US08524766B2

Reaction notes

Loading…