HCID 12172226, compound → HCID 59571145, compound

Participants

Reaction Steps

N,2,2-trimethylpent-4-en-1-amine (0.847 g, 6.66 mmol) was added to a solution of ethyl (2S)-2-isocyanatonon-8-enoate (1.50 g, 6.66 mmol) and THF (10 ml), and the solution aws stirred for 1 hour. The reaction mixture was concentrated and purified by silica gel chromatography (gradient elution, 20-30% EtOAc in hexane) to give the title compound. LRMS (M+1)=353.4.

Provenance & Evidence