HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 389236Generated: October 25, 2026
1,4-Dichlorobenzene → 1-(2-(2-Methoxyethoxy)ethyl)-2,3,3-trimethyl-3h-indolium bromide
https://huagongshe.com/reaction/389236
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,4-Dichlorobenzene | HCID 4685 | — |
| Reactant | 3H-Indole, 2,3,3-trimethyl- | HCID 15427 | — |
| Reactant | 1-Bromo-3,6-dioxaheptane | HCID 123532 | — |
| Product | 1-(2-(2-Methoxyethoxy)ethyl)-2,3,3-trimethyl-3h-indolium bromide | HCID 68813660 | — |
Reaction Steps
To 2,3,3-trimethylindolenine (1.59 g) was added 1-bromo-2-(2-methoxyethoxy)ethane (2.75 g) and dichlorobenzene (5 ml). The mixture was heated to 70° C. overnight. The volatiles were stripped and the material purified by HPLC.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08378120B2 |
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| Source dataset | uspto-grants-2013_02 |
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| ORD ID | ord-d7d322c6a96a4247a8c483bed3a38135 |
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| Source note | uspto-grants-2013_02 |
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