Triethylamine → HCID 58579973, compound

Participants

Reaction Steps

[3-(3-Aminomethyl-pyridin-2-yl)-4-methoxy-phenyl]-acetic acid methyl ester (0.140 g, 0.49 mmol) and triethylamine (0.17 mL, 1.23 mmol) was dissolved in CH2Cl2 (5 mL). Benzyl chloroformate (0.08 mL, 0.54 mmol) was added, and the reaction was stirred for 1 hour. Once no starting material was seen by analytical LCMS, the mixture was purified by preparative HPLC to give the title compound.

Provenance & Evidence