HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → 1-Acetoxy-3-(8,11,14-pentadecatrienyl) benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Cardanol | HCID 11266523 | — |
| Product | 1-Acetoxy-3-(8,11,14-pentadecatrienyl) benzene | HCID 69049096 | — |
Reaction Steps
A mixture of acetic anhydride (0.1 mol, 15 ml) and p-toluenesulphonic acid (PTSA, 3.15 mol %, 0.6 g) were taken in a two necked RB flask and double distilled cardanol (0.1 mol, 30 g) was added dropwise with stirring over a period of 30 minutes at ambient conditions. The reaction was continued for 8-12 h. The product (AC) was washed free of acetic acid and catalyst with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08378135B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-eef7ad41575b4ffdbb03c5667438d682 |
| Source note | uspto-grants-2013_02 |