HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 44470300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | [(2R)-5-chloro-7-(methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-yl]methyl 4-methylbenzenesulfonate | HCID 86652939 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 44470300 | HCID 44470300 | — |
Reaction Steps
Preparation according to Example 57 using [(2R)-5-chloro-7-(methylsulfonyl)-2,3-dihydro-1,4-benzodioxin-2-yl]methyl 4-methylbenzenesulfonate (0.027 g, 0.062 mmol), N-methylmethanamine (0.5 ml, 2.0 M in MeOH), ACN (3 ml). MS m/z (rel. intensity, 70 eV) 305 (M+, 0.4), 85 (2), 84 (3), 63 (2), 59 (4), 58 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524766B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-52735403f7b4420fa58c9a684ede71eb |
| Source note | uspto-grants-2013_09 |