HRID389599

反应详情

EQUATION

反应方程式

HRID 389599 的结构方程式

PROCEDURE

实验过程

The title compound was prepared from {7-[bis(tert-butoxycarbonyl)amino]-4-[1-(trans-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexyl)-1H-pyrazol-4-yl]furo[2,3-c]pyridin-2-yl}boronic acid and 7-bromo-1,2,3-benzothiadiazole-5-carbonitrile by a procedure analogous to Example 368. MS (ESI): 458.14 [M+H]+; HPLC tR=0.79 min (TOF: polar—2 min).

WORKUP

后处理

  1. customHPLC tR=0.79 min (TOF: polar—2 min)