HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → N-{[7-(Methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}prop-2-EN-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate | HCID 86652940 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-{[7-(Methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}prop-2-EN-1-amine | HCID 44470301 | — |
Reaction Steps
Preparation according to Example 25: [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate (0.020 g, 0.0504 mmol), prop-2-en-1-amine (0.5 ml), ACN (3 ml). MS m/z (rel. intensity, 70 eV) 281 (M+, 6), 131 (8), 77 (6), 71 (5), 70 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524766B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-b74d61c491c042adb307e542f6aebcdb |
| Source note | uspto-grants-2013_09 |