HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Piperidone → HCID 67155298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Piperidone | HCID 12665 | — |
| Reactant | HCID 67155224 | HCID 67155224 | — |
| Product | HCID 67155298 | HCID 67155298 | — |
Reaction Steps
Intermediate 35 (4 g, 12.06 mmol) was coupled with piperidin-2-one (1.434 g, 14.47 mmol) in close analogy to the procedure described in step 1.6). After workup the crude oil is purified by chromatography on silica gel (n-heptane-ethyl acetate 4:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08378092B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-b96a8bb7a4254ec488798e1e20fe91c3 |
| Source note | uspto-grants-2013_02 |