HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dipropylamine → N-{[7-(Methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}-N-propylpropan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dipropylamine | HCID 8902 | — |
| Reactant | [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate | HCID 86652940 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N-{[7-(Methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}-N-propylpropan-1-amine | HCID 44468513 | — |
Reaction Steps
Preparation according to Example 25: [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate (0.020 g, 0.0504 mmol), N-propylpropan-1-amine (0.5 ml), ACN (3 ml). MS m/z (rel. intensity, 70 eV) 325 (M+, 1), 296 (7), 131 (4), 115 (10), 114 (bp), 86 (6).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524766B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-115a309523ce46fd8dc9390864734267 |
| Source note | uspto-grants-2013_09 |