1-Propanamine, N-ethyl- → N-Ethyl-N-{[7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}propan-1-amine

Participants

Role	Name	HCID	Charge
Reactant	1-Propanamine, N-ethyl-	HCID 88398	—
Reactant	[7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate	HCID 86652940	—
Solvent	Acetonitrile	HCID 6342	—
Product	N-Ethyl-N-{[7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-YL]methyl}propan-1-amine	HCID 44468512	—

Reaction Steps

Preparation according to Example 25: [7-(methylsulfonyl)-3,4-dihydro-2H-chromen-2-yl]methyl 4-methylbenzenesulfonate (0.020 g, 0.0504 mmol), N-ethylpropan-1-amine (0.5 ml), ACN (3 ml). MS m/z (rel. intensity, 70 eV) 311 (M+, 1), 282 (5), 101 (8), 100 (bp), 72 (6), 58 (9).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08524766B2
Source dataset	uspto-grants-2013_09
ORD ID	ord-ca59e52c68d74e00b761c37003e3cb1f
Source note	uspto-grants-2013_09