HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Chlorothio)formyl chloride → 5-(3-Chlorobenzyl)-1,3,4-oxathiazol-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Chlorothio)formyl chloride | HCID 75990 | — |
| Reactant | 2-(3-Chlorophenyl)acetamide | HCID 5324746 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 5-(3-Chlorobenzyl)-1,3,4-oxathiazol-2-one | HCID 67079857 | — |
Reaction Steps
7.32 g (55.9 mmol) of chlorocarbonylsulphenyl chloride and 7.90 g (46.6 mmol) of 2-(3-chlorophenyl)acetamide are stirred in 50 ml of toluene at 80° C. for 3 h. The crude product is reacted further without additional purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383139B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-aed017e578454e8ba2dc5d75ba928ed7 |
| Source note | uspto-grants-2013_02 |