Triethyl phosphite → HCID 178476838, compound

HRID 389836Notes

Reaction equation

HRID 389836 reaction equation
[Cl-].[CH3:2][O:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]([C:12]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:13])=[O:11])=[CH:6][CH:5]=1.[P:20]([O:27]CC)([O:24][CH2:25][CH3:26])[O:21][CH2:22][CH3:23]>>[CH2:22]([O:21][PH:20](=[O:27])[O:24][CH2:25][CH3:26])[CH3:23].[CH3:2][O:3][C:4]1[CH:5]=[CH:6][C:7]([C:10]([C:12]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:13])=[O:11])=[CH:8][CH:9]=1

Participants

3

Reactant 2

HCID 31215Triethyl phosphiteHCID 86650128HCID 86650128, compound

Product 1

HCID 178476838HCID 178476838, compound

Procedure

156.6 parts of 4-methoxy benzil chloride and 332.0 parts of triethyl phosphite are reacted at 150° C. for 5 hours.

Sources & evidence

ORD record
ord-4d380c46c8ec4a7db634d6267b0bb356
Source dataset
uspto-grants-2013_02
Patent number
US08383305B2

Reaction notes

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