Potassium Carbonate → 3-amino-1-[{4-(2,3-dimethylphenyl)piperazin-1-yl}propanoyl]-6-N-(p-tolyl)-4,5,6,7-tetrahydro-1H-pyrazolo[3,4-c]pyridin-7-one

Participants

Reaction Steps

A target compound (80.9 mg, 0.166 mmol, 47.5%) was yielded as white solid in the same manner as Example 1 by reacting 1-N-t-butoxycarbonyl-3-amino-4,5,6,7-tetrahydro-6-N-(p-tolyl)pyrazolo[3,4-c]pyridin-7-one (120 mg, 0.350 mmol) with potassium carbonate (53.2 mg, 0.385 mmol) and 3-chloro-1-(4-(2,3-dimethylphenyl)piperazin-1-yl)propan-1-one (103.0 mg, 0.367 mmol).

Provenance & Evidence