HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → 4-[(Trifluoromethyl)sulfonyl]phenyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 4-Trifluoromethanesulfonylphenol | HCID 14857426 | — |
| Product | 4-[(Trifluoromethyl)sulfonyl]phenyl acetate | HCID 67200435 | — |
Reaction Steps
Preparation according to Preparation 16 using 4-[(trifluoromethyl)sulfonyl]phenol (4.5 g, 23.2 mmol), acetic anhydride (13.4 g, 130 mmol) and pyridine (10.6 ml, 130 mmol). Crude yield: 6.8 g. MS m/z (rel. intensity, 70 eV) 268 (M+, 6), 157 (bp), 93 (84), 65 (52), 64 (43).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08524766B2 |
| Source dataset | uspto-grants-2013_09 |
| ORD ID | ord-a06679e2163f43058595564df9b2cbc6 |
| Source note | uspto-grants-2013_09 |