HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3,5-Dichloro-2-iodobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3,5-dichloro-2-iodo-benzoic Acid | HCID 3843298 | — |
| Product | 3,5-Dichloro-2-iodobenzoyl chloride | HCID 14174372 | 98% |
Reaction Steps
A mixture of 3,5-dichloro-2-iodo-benzoic acid (9.0 g, 28 mmol) and SOCl2 (100 mL) was heated to reflux overnight. The solvent was removed to give crude 3,5-dichloro-2-iodobenzoyl chloride (9.4 g, 98%). 1H NMR (CDCl3): 7.64 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383629B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-34340bce77d843f0b9c306c31f6a474b |
| Source note | uspto-grants-2013_02 |