Cyclohexanecarboxaldehyde → HCID 58625082, compound

Participants

Reaction Steps

The reaction was completed under N2. Cyclohexanecarboxaldehyde (0.01 mol) and then NaBH(OAc)3 (0.015 mol) were added to a solution of 3-(3-dimethoxymethyl-4-nitro-phenoxy)-phenylamine (0.01 mol) in DCE (130 mL). The reaction mixture was stirred overnight at room temperature and washed with a saturated NaHCO3 solution. The organic layer was separated, dried (MgSO4) and filtered, and the solvent was evaporated to yield the title compound as a residue.

Provenance & Evidence