HRID390377

反应详情

EQUATION

反应方程式

HRID 390377 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Pyridine-3,5-dicarboxylic acid dimethyl ester (5.3 g, 27 mmol) and Rh/PtO2 (0.5 g) in MeOH (200 mL) are stirred under hydrogen overnight. The resulting mixture is filtered and the solvents are evaporated to give a brown oil. MS (LC-MS): 202 [M+H]+

WORKUP

后处理

  1. filtrationThe resulting mixture is filtered
  2. customthe solvents are evaporated
  3. customto give a brown oil