Ammonia → HCID 44546224, compound

Participants

Reaction Steps

The titled compound was prepared as the hydrochloride salt according to Method CB using the product of Example 1A (78 mg, 0.5 mmol) and 1-chloro-4-ethynylbenzene (Aldrich, 68 mg, 0.5 mmol). 1H NMR (300 MHz, DMSO-d6) δ 7.62-7.75 (m, 3H), 7.79 (s, 1H), 7.89-8.01 (m, 2H), 8.40 (dt, J=8.1, 1.7 Hz, 1H), 8.78 (dd, J=5.1, 1.4 Hz, 1H), 9.16 (d, J=2.0 Hz, 1H) ppm; MS (DCI/NH3) m/z 259 (M+H)+, 257 (M+H)+.

Provenance & Evidence