HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 44546483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | p-Ethynyltoluene | HCID 13018 | — |
| Reactant | N-Hydroxypyrimidine-5-carbimidoyl chloride | HCID 86636847 | — |
| Product | HCID 44546483 | HCID 44546483 | — |
Reaction Steps
The titled compound was prepared as the hydrochloride salt according to Method CB using the product of Example 44B (79 mg, 0.5 mmol) and 1-ethynyl-4-methylbenzene (Apollo, 58 mg, 0.5 mmol). 1H NMR (300 MHz, DMSO-d6) δ 2.40 (s, 3H), 7.42 (d, J=8.1 Hz, 2H), 7.70 (s, 1H), 7.81 (d, J=8.5 Hz, 2H), 9.32 (s, 2H), 9.34 (s, 1H) ppm; MS (DCI/NH3) m/z 238 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383658B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-f4d2cbcfaf9a48829206e818c0e014da |
| Source note | uspto-grants-2013_02 |