反应详情

The titled compound was prepared according to Method CB using the product of Example 69B (57 mg, 0.3 mmol) and 1,2-dichloro-4-ethynylbenzene (Aldrich, 51 mg, 0.3 mmol). 1H NMR (300 MHz, DMSO-d6) δ 7.89 (d, J=1.2 Hz, 2H), 7.93 (s, 1H), 8.18 (s, 1H), 8.40-8.44 (m, 1H), 8.82 (d, J=2.4 Hz, 1H), 9.06 (d, J=2.0 Hz, 1H) ppm; MS (DCI/NH3) m/z 325 (M+H)+, 327 (M+H)+, 329 (M+H)+.