反应详情

The titled compound was prepared according to Method CB using the product of Example 69B (57 mg, 0.3 mmol) and 1-ethynyl-3,5-difluorobenzene (Apollo, 41 mg, 0.3 mmol). 1H NMR (300 MHz, DMSO-d6) δ 7.51 (tt, J=9.3, 2.4 Hz, 1 H), 7.61-7.74 (m, 2H), 7.93 (s, 1H), 8.41 (t, J=2.1 Hz, 1H), 8.82 (d, J=2.4 Hz, 1 H), 9.06 (d, J=1.7 Hz, 1H) ppm; MS (DCI/NH3) m/z 293 (M+H)+, 295 (M+H)+.