反应详情

The titled compound was prepared according to Method CB using the product of Example 83D (79 mg, 0.5 mmol) and 1-ethynyl-benzene (Aldrich, 52 mg, 0.5 mmol). 1H NMR (300 MHz, MeOH-d4) δ 7.41 (s, 1H), 7.47-7.70 (m, 3H), 7.86-8.08 (m, 2H), 8.70 (d, J=2.4 Hz, 1H), 8.76 (dd, J=2.8, 1.6 Hz, 1H), 9.29 (d, J=1.2 Hz, 1H) ppm; MS (DCI/NH3) m/z 224 (M+H)+.