反应详情

The titled compound was prepared according to Method CB using the product of Example 83D (79 mg, 0.5 mmol) and 1-ethynyl-3-fluorobenzene (Aldrich, 60 mg, 0.5 mmol). 1H NMR (300 MHz, MeOH-d4) δ 7.19-7.33 (m, 1H), 7.48 (s, 1 H), 7.58 (td, J=8.1, 5.8 Hz, 1H), 7.69 (dt, J=9.6, 2.2 Hz, 1H), 7.77 (dt, J=8.0, 1.1 Hz, 1H), 8.70 (d, J=2.4 Hz, 1H), 8.76 (dd, J=2.4, 1.7 Hz, 1H), 9.29 (d, J=1.4 Hz, 1H) ppm; MS (DCI/NH3) m/z 242 (M+H)+.