HCID 57748176, compound → HCID 86631931, compound
Reaction equation
Cl.[NH2:2][C:3]1[CH:4]=[CH:5][C:6]([Cl:9])=[N:7][CH:8]=1.[S:10]([CH:13]([CH3:16])[CH:14]=O)[C:11]#[N:12]>>[ClH:9].[Cl:9][C:6]1[N:7]=[CH:8][C:3]([N:2]2[CH:14]=[C:13]([CH3:16])[S:10][C:11]2=[NH:12])=[CH:4][CH:5]=1Participants
3
Procedure
The title compound was prepared from 5-amino-2-chloropyridine hydrochloride and 2-thiocyanatopropanal as described for Example 160A. The title compound was used without additional purification.
Workup
- customThe title compound was used without additional purification
Sources & evidence
- ORD record
- ord-f06cde1e5dea46159cdcb8e874c5031b
- Source dataset
- uspto-grants-2013_02
- Patent number
- US08383657B2
Reaction notes
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