huagongshe.com
HRID390941

反应详情

EQUATION

反应方程式

HRID 390941 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OB(c2ccc(N)nc2)OC1(C)C
HCID2756555

5-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-amine

C11H17BN2O2

结构：CS(=O)(=O)N1CCN(Cc2cc3nc(Cl)nc(N4CCOCC4)c3o2)CC1
HCID56833744

未命名化合物

PRODUCTS

生成物

1
结构：CS(=O)(=O)N1CCN(Cc2cc3nc(-c4ccc(N)nc4)nc(N4CCOCC4)c3o2)CC1
HCID58233946

未命名化合物

PROCEDURE

实验过程

2-Chloro-6-((4-(methylsulfonyl)piperazin-1-yl)methyl)-4-morpholinofuro[3,2-d]pyrimidine was reacted with 5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-amine via General Procedure E to give, after purification by reverse HPLC, 22 mg of 236. MS (Q1) 474 (M+).

WORKUP

后处理

  1. customto give
  2. customafter purification by reverse HPLC, 22 mg of 236