HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → 2-(2,5-Dibromophenyl)benzo[d]thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | 2-Aminothiophenol | HCID 8713 | — |
| Reactant | 2,5-Dibromobenzaldehyde | HCID 13540069 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-(2,5-Dibromophenyl)benzo[d]thiazole | HCID 58479963 | — |
Reaction Steps
5 g (18.5 mmol) of 2,5-dibromobenzaldehyde, 3 mL (27.7 mmol) of 2-aminothiophenol, and 2.35 g (9.25 mmol) of iodine (I2) were dissolved in 100 mL of DMF. The solution was reacted at 100° C. for 1 hour. The acquired reactant was purified through a column, obtaining 4.64 g (Y=68%) of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383932B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-f96d9b3d41124928b08d26b4482b5346 |
| Source note | uspto-grants-2013_02 |