HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1-chloro-4-ethynyl- → HCID 24952434, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1-chloro-4-ethynyl- | HCID 70118 | — |
| Reactant | (S)-5-bromo-N-[methyl(oxido)phenyl--sulfanylidene]nicotinamide | HCID 86629466 | — |
| Product | HCID 24952434 | HCID 24952434 | 49% |
Reaction Steps
In a manner similar to that describe in Example 425 a mixture of (S)-5-bromo-N-[methyl(oxo)phenyl-λ6-sulfanylidene]nicotinamide and 4-chloro-1-ethynylbenzene were reacted to give the title compound as white needles (60 mg, 49%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383825B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-515209c14c6d4bb3a17295e5154c8a77 |
| Source note | uspto-grants-2013_02 |