HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamic acid, (4-ethynylphenyl)-, 1,1-dimethylethyl ester (9CI) → HCID 24953488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamic acid, (4-ethynylphenyl)-, 1,1-dimethylethyl ester (9CI) | HCID 12121165 | — |
| Reactant | 5-bromo-N-[methyl(oxo)phenyl-lambda6-sulfanylidene]nicotinamide | HCID 57657819 | — |
| Product | HCID 24953488 | HCID 24953488 | 45% |
Reaction Steps
In a manner similar to that described in Example 449, tert-butyl 4-ethynylphenylcarbamate (0.096 g, 0.443 mmol) and 5-bromo-N-[methyl(oxo)phenyl-λ6-sulfanylidene]nicotinamide (100 mg, 0.295 mmol) were reacted to give the title compound as a solid (63 mg, 0.13 mmol, 45%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08383825B2 |
| Source dataset | uspto-grants-2013_02 |
| ORD ID | ord-e3f2d874c9034f9088a6b1e43e2d31a4 |
| Source note | uspto-grants-2013_02 |