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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 391582Generated: October 30, 2026

Potassium Carbonate → Methyl 3-[4-(S-methylsulfonimidoyl)phenyl]propanoate

https://huagongshe.com/reaction/391582

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantMethyl 3-{4-[S-methyl-N-(trifluoroacetyl)sulfonimidoyl]phenyl}-propanoateHCID 57657821—
SolventMethanolHCID 887—
ProductMethyl 3-[4-(S-methylsulfonimidoyl)phenyl]propanoateHCID 5765782293.3%

Reaction Steps

Methyl 3-{4-[S-methyl-N-(trifluoroacetyl)sulfonimidoyl]phenyl}propanoate (0.200 g, 0.653 mmol) was dissolved in MeOH (3 mL). K2CO3 (0.450 g, 3.27 mmol) was added to the solution, and the resulting suspension was allowed to stir for 5 minutes. The suspension was filtered and the filtrate was concentrated. The residue was dissolved in EtOAc and dried over anhydrous anhydrous Na2SO4(s) to give the title compound (0.147 g, 93%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08383825B2
Source datasetuspto-grants-2013_02
ORD IDord-51dab07d77ba41a885011de6cd0223f2
Source noteuspto-grants-2013_02