反应详情

温度

60 °C

4,4′-Dimethoxybenzhydrol (2.7 g, 11 mmol) and 4-mercaptophenylboronic acid (1.54 g, 10 mmol) were dissolved in AcOH (20 mL) and heated at 60° C. for 1 h. Solvent was evaporated and the residue was dried under high vacuum. This material was used without further purification.

1. customSolvent was evaporated
2. customthe residue was dried under high vacuum
3. customThis material was used without further purification