Sodium Cyanide → HCID 69365399, compound

HRID 392152Notes

Reaction equation

HRID 392152 reaction equation
Br[CH2:2][CH2:3][C:4]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=2[O:6][CH:5]=1.[C-:13]#[N:14].[Na+]>>[O:6]1[C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=2[C:4]([CH:3]([CH3:2])[C:13]#[N:14])=[CH:5]1

Participants

3

Reactant 2

HCID 8929Sodium CyanideHCID 150754803-(2-bromoethyl)Benzofuran

Product 1

HCID 69365399HCID 69365399, compound

Procedure

This compound was prepared by the same method as for intermediate 27, using 1.98 g (8.8 mmol) of 3-(2-bromoethyl)benzofuran and 0.86 g (17.6 mmol) of NaCN, to afford 1.5 g (quant.) of the title compound: MS (ESI) m/z 171 [M]+.

Sources & evidence

ORD record
ord-a6527e88c46c4e8fabf84d21e2933435
Source dataset
uspto-grants-2004_10
Patent number
US06800637B2

Reaction notes

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