HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-Enal → (E,E)-2-(benzylaminocarbonyl)-3-styrylacrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-Enal | HCID 307 | — |
| Reactant | N-(cyanoacetyl)benzylamide | HCID 178511179 | — |
| Product | (E,E)-2-(benzylaminocarbonyl)-3-styrylacrylonitrile | HCID 5835419 | — |
Reaction Steps
The compound was prepared as described in Example 3 by adding cinnamaldehyde (0.048 ml, 0.38 mmol) to N-(cyanoacetyl)benzylamide (Example 4, 0.066 g, 0.38 mmol). After refluxing for 1 h and recrystallization from ethanol a white solid was obtained (0.074 g, 68%). The product gave the following analytical data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06800659B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-362fc3e8426c48ebb32387ada05775b4 |
| Source note | uspto-grants-2004_10 |