Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(3,4-Dimethoxyphenyl)-2-propenal → (E,E)-2-(Phenylethylaminocarbonyl)-3-(3,4-dimethoxystyryl)acrylonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(3,4-Dimethoxyphenyl)-2-propenal | HCID 107557 | — |
| 반응물 | HCID 178511181 | HCID 178511181 | — |
| 생성물 | (E,E)-2-(Phenylethylaminocarbonyl)-3-(3,4-dimethoxystyryl)acrylonitrile | HCID 10109276 | — |
반응 단계
The compound was prepared as described in Example 3 by adding 3,4-dimethoxycinnamaldehyde (Example 6, 0.1 g, 0.52 mmol) to N-(cyanoacetyl)phenylethylamide (Example 20, 0.1 g, 0.52 mmol). After refluxing for 1 h and recrystallization from ethanol a yellow solid was obtained (0.12 g, 63%). The product gave the following analytical data:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06800659B2 |
| 출처 데이터셋 | uspto-grants-2004_10 |
| ORD ID | ord-3c2519fed33b4ecba3aefc797ac7d1b3 |
| 출처 메모 | uspto-grants-2004_10 |