HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetic acid → (E,E)-2-Carboxy-3-(3,5-dimethoxy-4-hydroxystyryl)acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetic acid | HCID 9740 | — |
| Reactant | 2-Propenal, 3-(4-hydroxy-3,5-dimethoxyphenyl)- | HCID 119216 | — |
| Product | (E,E)-2-Carboxy-3-(3,5-dimethoxy-4-hydroxystyryl)acrylonitrile | HCID 9965375 | — |
Reaction Steps
The compound was prepared as described in Example 3 by adding 3,5-dimethoxy-4-hydroxycinnamaldehyde (0.15 g, 0.72 mmol) to cyanoacetic acid (0.061 g, 0.72 mmol). After refluxing for 1 h and recrystallization from ethanol a yellow solid was obtained (0.15 g, 75%). The product gave the following analytical data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06800659B2 |
| Source dataset | uspto-grants-2004_10 |
| ORD ID | ord-78ad4023914a4c638fdec8547058e4e6 |
| Source note | uspto-grants-2004_10 |