Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(4-Nitrophenyl)prop-2-enal → (E,E)-2-(Benzylaminocarbonyl)-3-(4-nitrostyryl)acrylonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(4-Nitrophenyl)prop-2-enal | HCID 15614 | — |
| 반응물 | N-(cyanoacetyl)benzylamide | HCID 178511179 | — |
| 생성물 | (E,E)-2-(Benzylaminocarbonyl)-3-(4-nitrostyryl)acrylonitrile | HCID 9858847 | 82.5% |
반응 단계
The compound was prepared as described in Example 3 by adding 4-nitrocinnamaldehyde (0.022 g, 0.12 mmol) to N-(cyanoacetyl)benzylamide (Example 4, 0.022 g, 0.12 mmol). After refluxing for 1 h, the product was purified by silica gel chromatography (CHCl3-MeOH, 5:1) to give a yellow solid (0.033 g, 81%) The product gave the following analytical data:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06800659B2 |
| 출처 데이터셋 | uspto-grants-2004_10 |
| ORD ID | ord-4be7cbb7f1b7495ca26935f24b73548b |
| 출처 메모 | uspto-grants-2004_10 |