HRID392560

反应详情

EQUATION

反应方程式

HRID 392560 的结构方程式

PROCEDURE

实验过程

The title compound is prepared according to the procedure of Example 23 using 45 g of 2,4-di-(4-chloro-α-cumyl)phenol prepared in Example 6 and 138 g of the diazonium salt solution prepared in Example 11 in a yield of 66.3 g. The desired product is a crimson red solid containing some residual salt and melts at 163-165° C. The structure is confirmed by 1Hnmr and mass spectroscopy analyses.

WORKUP

后处理

  1. customThe title compound is prepared
  2. additioncontaining some residual salt and melts at 163-165° C