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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 392564Generated: October 30, 2026

N,N-Dimethylethylenediamine → HCID 22664376, compound

https://huagongshe.com/reaction/392564

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN,N-DimethylethylenediamineHCID 66053—
ReactantHCID 22664396HCID 22664396—
ProductHCID 22664376HCID 22664376—

Reaction Steps

The title compound is prepared according to the procedure given in instant Example 35 using 8.0 g of the intermediate compound prepared in Example 34a and 1.4 g of 2-dimethylaminoethylamine. After several recrystallizations from ethyl acetate and ethyl acetate/heptane mixtures, 5.6 g of the title compound is prepared as a near white solid melting at 118-120° C. The structure of the compound is confirmed by 1Hnmr and mass spectroscopy analyses.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06800676B2
Source datasetuspto-grants-2004_10
ORD IDord-b9bfd375883e47c38c8c2137aa3d8f9a
Source noteuspto-grants-2004_10