tert-Butanol → HCID 11066908, compound

HRID 392690Notes

Reaction equation

[C:1]1([CH:7]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[C:8]([N:10]=[C:11]=[O:12])=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:19]([OH:23])([CH3:22])([CH3:21])[CH3:20]>>[C:19]([O:23][C:11](=[O:12])[NH:10][C:8](=[O:9])[CH:7]([C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)([CH3:22])([CH3:21])[CH3:20]

Participants

Reactant 2

HCID 6386tert-Butanol

HCID 11264874Diphenylacetyl isocyanate

Product 1

HCID 11066908HCID 11066908, compound

Procedure

The title compound, light yellow solid, m.p. 160-162° C. and MS: m/e=334 (M+Na+) was prepared in accordance with the general method of example 1 from diphenylacetyl isocyanate and tert.-butyl alcohol.

Sources & evidence

ORD record: ord-eaf8b37cb5bf4bbdaef21b2547ac1775
Source dataset: uspto-grants-2004_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06803381B1

Reaction notes

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