Carbamic acid, ethyl ester → HCID 54072216, compound

HRID 392692Notes

Reaction equation

HRID 392692 reaction equation
[NH2:1][C:2]([O:4][CH2:5][CH3:6])=[O:3].[Br:7][C:8]1[CH:21]=[CH:20][C:19]2[O:18][C:17]3[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=3)[CH:11]([C:22](Cl)=[O:23])[C:10]=2[CH:9]=1>>[CH2:5]([O:4][C:2](=[O:3])[NH:1][C:22]([CH:11]1[C:10]2[CH:9]=[C:8]([Br:7])[CH:21]=[CH:20][C:19]=2[O:18][C:17]2[C:12]1=[CH:13][CH:14]=[CH:15][CH:16]=2)=[O:23])[CH3:6]

Participants

3

Reactant 2

HCID 5641Carbamic acid, ethyl esterHCID 22661081HCID 22661081, compound

Product 1

HCID 54072216HCID 54072216, compound

Procedure

The title compound, light brown solid, m.p. 203° C. and MS: m/e=375 (M+) was prepared in accordance with the general method of example 6 from urethane and 2-bromo-9H-xanthene-9-carbonyl chloride.

Sources & evidence

ORD record
ord-dfa0df83a2074d8ca94b738e10e83912
Source dataset
uspto-grants-2004_10
Patent number
US06803381B1

Reaction notes

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